Clay composition patterns and their influence on the adhesive strength of earthen plasters

Authors

  • Gonzalo García Villar Consejo Nacional de Investigaciones Científicas y Técnicas (CONICET), Centro Regional de Investigaciones de Arquitectura de Tierra Cruda (CRIATiC), Facultad de Arquitectura y Urbanismo (FAU), Universidad Nacional de Tucumán (UNT), Tucumán (Argentina)
  • Marcial Enzo Consejo Nacional de Investigaciones Científicas y Técnicas (CONICET), Instituto Superior de Correlación Geológica (INSUGEO), Centro Integral de Microscopía Electrónica (CIME), Universidad Nacional de Tucumán (UNT), Tucumán (Argentina)
  • Rolón Guillermo Consejo Nacional de Investigaciones Científicas y Técnicas (CONICET), Instituto de Investigaciones Territoriales y Tecnológicas para la Producción del Habitat (InTePH), Facultad de Arquitectura y Urbanismo (FAU), Universidad Nacional de Tucumán (UNT), Tucumán, (Argentina)

DOI:

https://doi.org/10.7764/RDLC.23.1.71

Keywords:

Shear test, pull-off test, granulometric compensation, physiographic units, mineralogical composition.

Abstract

The clay fraction of earthen plasters is the part responsible for the acquisition of cohesion and adherence that they possess against deterioration factors. Adherence is the property responsible for keeping the plaster together with the wall and is influenced by the percentage content of clay as well as by its mineralogy and the heterogeneity of minerals that may be present. However, it is still unknown in depth how clay minerals perform in the adherent properties of earthen plasters when the composition is heterogeneous in the material. The objective of this study is to evaluate the incidence of the mineralogical complexity of clay mineralogy in the variability of the adherence of earth plasters. To evaluate the variability, considering that the mineralogy of the soils depends directly on the place and the formation processes, eight soils from Tucumán (Argentina) corresponding to different physiographic units were analyzed. A methodology was designed for sample preparation that allows soils to be compared through adhesion tests. They were characterized by XRD to determine their mineralogical composition and by the hydrometric method to determine their granulometry. To evaluate the adherence of mixtures made with the respective soils, it was proposed in the first instance to compensate the granulometry of the soils to equate them and, once the plasters were made, this property was evaluated through shear and pull-off tests. The results showed that they allowed us to identify that the soils presented a pattern of mineralogical composition common to all the physiographic units, made up of the Ill and K pair, the former being predominant. For this pattern, it was observed in particular that there is a positive correlation between the increase in Ill content with the increase in the adhesive strength of the plasters. Clay minerals from the Sm group also contribute to the increase in adherence when the percentage is greater than or equal to 11%. On the contrary, K and Cl do not influence the increase in adhesive strength.The clay fraction of earthen plasters is the part responsible for the acquisition of cohesion and adherence that they possess against deterioration factors. Adherence is the property responsible for keeping the plaster together with the wall and is influenced by the percentage content of clay as well as by its mineralogy and the heterogeneity of minerals that may be present. However, it is still unknown in depth how clay minerals perform in the adherent properties of earthen plasters when the composition is heterogeneous in the material. The objective of this study is to evaluate the incidence of the mineralogical complexity of clay mineralogy in the variability of the adherence of earth plasters. To evaluate the variability, considering that the mineralogy of the soils depends directly on the place and the formation processes, eight soils from Tucumán (Argentina) corresponding to different physiographic units were analyzed. A methodology was designed for sample preparation that allows soils to be compared through adhesion tests. They were characterized by XRD to determine their mineralogical composition and by the hydrometric method to determine their granulometry. To evaluate the adherence of mixtures made with the respective soils, it was proposed in the first instance to compensate the granulometry of the soils to equate them and, once the plasters were made, this property was evaluated through shear and pull-off tests. The results showed that they allowed us to identify that the soils presented a pattern of mineralogical composition common to all the physiographic units, made up of the Ill and K pair, the former being predominant. For this pattern, it was observed in particular that there is a positive correlation between the increase in Ill content with the increase in the adhesive strength of the plasters. Clay minerals from the Sm group also contribute to the increase in adherence when the percentage is greater than or equal to 11%. On the contrary, K and Cl do not influence the increase in adhesive strength.

References

ASTM D422-63 (2007) Standard Test Method for Particle-Size Analysis of Soils. ASTM Internacional

Bueno Buelvas R & Fernández Lizarazo JC (2019) La capacidad de intercambio catiónico del suelo: una bóveda de nutrición clave en la producción de alimentos. Ámbito investigativo, 4(1): 7-12. https://ciencia.lasalle.edu.co/ai

Bouyoucos GJ. (1962) Hydrometer method for making particle size analysis de soils, Agronomy Journal, 54: 464-465, https://doi.org/10.2134/agronj1962.00021962005400050028x

BS EN 1015-12 (2000) Methods of test for mortar for masonry

Callister, W., & Rethwisch, D. (2014). Materials science and engineering. An Introduction (Wiley (ed.); 9th Edition).

Cavicchioli A, Rolón G & Odlyha M (2022) A Chemical Approach to the Selection of Soils for the Reproduction of Earth-based Mortars for Conservation Purposes: Case Report from a Brazilian Historic Site, International Journal of Architectural Heritage. https://doi.org/10.1080/15583058.2022.2086504.

Christidis GE (2011) Industrial Clays, Chapter in European Mineralogical Union Notes in Mineralogy. doi: 10.1180/EMU-notes.9.9

Costa CS, Rocha E, Varum H & Velosa A (2013) Influence of the mineralogical composition on the properties of adobe blocks from Aveiro, Portugal. Clay Minerals, 48: 749–758 https://doi:10.1180/claymin.2013.048.5.07

Delinière R, Aubert JE, Rojat F & Gasc-Barbier M (2014) Physical, mineralogical and mechanical characterization of ready-mixed clay plaster, Build. Environ. 80:11–17. doi: 10.1016/j.buildenv.2014.05.012

DIN 18947 (2013) Lehmputzmörtel - Begriffe, Anforderungen und Prüfverfahren

Duarte I, Pedro E, Varum H & Mirao J (2015) Soil mineralogical composition effects on the durability of adobe blocks from the Huambo region, Angola, Bulletin of Engineering Geology and the Environment 76(1): 125-132 https://doi:10.1007/s10064-015-0800-3

Ekosse E (2010) Kaolin deposits and occurrences in Africa: Geology, mineralogy, and utilization. Applied Clay Science, 50(2): 212–236. https://doi:10.1016/j.clay.2010.08.003

Elert K (2014) Alkaline activation of clays for the consolidation of earthen architecture, Tesis Doctoral, Universidad de Granada

Elert K, Jroundi F, Benavides-Reyes C, Correa Gómez E, Gulotta D & Rodriguez-Navarro C (2022) Consolidation of clay-rich earthen building materials: A comparative study at the Alhambra fortress (Spain), Journal of Building Engineering, 50: 104081 https://doi.org/10.1016/j.jobe.2022.104081

Faria P, Lima J, Nabais J, Silva V (2019) Assessment of adhesive strength of an earth plaster on different substrates through different methods. In Proceedings pro130: 5th Historic Mortars Conference HMC2019. Pamplona, Spain: RILEM Publications SARL. Pp. 51-65. https://www.rilem.net/publication/publication/49

Fernández DS, Lutz MA, García MG, Hidalgo M, Pereyra F & Tchilinguirian P (2008) Carta de Líneas de Base Ambiental 2766-IV -San Miguel de Tucumán-, provincias de Tucumán, Salta, Santiago del Estero y Catamarca. Servicio Geológico Minero Argentino (Eds.). Buenos Aires. Boletin Nº 374

Fratini F, Pecchioni E, Rovero L & Tonietti U (2011) The earth in the architecture of the historical center of Lamezia Terme (Italy): Characterization for restoration, Applied Clay Science. 53: 509-516 https://doi:10.1016/j.clay.2010.11.007

García Villar G (2022) Evaluación de la adherencia de capas de agarre para revoques de tierra sobre paredes de técnica mixta. Seminario Iberoamericano de Arquitectura y Construcción con Tierra, 20. Memorias.Trinidad, Cuba: PROTERRA/Oficina del Conservador. 210-219. https://redproterra.org/wp-content/uploads/2022/04/20-SIACOT-Cuba-2022-web.pdf.

Guerrero Baca LF (2007) Arquitectura en tierra. Hacia la recuperación de una cultura constructiva. Journal of Cultural Heritage Studies, Vol. 20-2: 182-201

Hamard E, Morel JC, Salgado F, Marcom A & Meunier N (2013) A procedure to assess the suitability of plaster to protect vernacular earthen architecture, J. Cult. Heritage 14 (2): 109–115. https://doi.org/10.1016/j.culher.2012.04.005

Houben H, Guillaud H (2008) Earth construction: A comprehensive guide. CRAterre, Intermediate Technology Publications. Practical Action Publishing, Warwickshire (Eds.)

Huggett J (2013) Clay Minerals. Reference Module in Earth Systems and Environmental Sciences. doi: 10.1016/B978-0-12-409548-9.09519-1

IPC,Instituto de promoción cerámica (2022). http://www.ipc.org.es/guia_colocacion/info_tec_colocacion/mat_agarre/adherencia.html, (accessed 22 December 2022)

IRAM 1764 (2013) Método de ensayo de adherencia de los revoques y las carpetas

Jia, Q., Chen, W., & Tong, Y. (2024). Influence of material composition on physical performance of earthen plasters. Construction and Building Materials, 417, 135219. https://doi.org/10.1016/j.conbuildmat.2024.135219

Lagouin M, Aubert JE, Laborel-Préneron A & Magniont C (2021a) Influence of chemical, mineralogical and geotechnical characteristics of soil on earthen plaster properties, Constructions and Building Materials, 304: 124339. https://doi.org/10.1016/j.conbuildmat.2021.124339

Lagouin M, Laborel-Préneron A, Magniont C, Geoffroy S & Aubert SE (2021b) Effects of organic admixtures on the fresh and mechanical properties of earth-based plasters, Journal of building engineering 41304:102379, https://doi.org/10.1016/j.jobe.2021.102379

Lima J, Faria P & Santos Silva A (2016) Earthen Plasters Based on Illitic Soils from Barrocal Region of Algarve: Contributions for Building Performance and Sustainability, Key Engineering Materials,678: 64-77. doi:10.4028/www.scientific.net/KEM.678.64. http://www.scientific.net/KEM.678.64

Lima J, Faria P & Santos Silva A (2020) Earth Plasters: The Influence of Clay Mineralogy in the Plasters’ Properties. International Journal of Architectural Heritage. 1–16. doi: 10.1080/15583058.2020.1727064

Meimaroglou N & Mouzakis C (2019) Cation Exchange Capacity (CEC), texture, consistency and organic matter in soil assessment for earth construction: The case of earth mortars. Constructions and Building Materials 221: 27–39 https://doi.org/10.1016/j.conbuildmat.2019.06.036

Minke G (2000) Earth construction handbook, in The building material earth in modern architecture., WIT Press ed., Southampton and Boston

Mitchell K & Soga K (2005) Soil Mineralogy, in Fundamentals of Soil Behavior, 3rd Edition, John Wiley & Sons, Ltd, pp. 592

Moore DM & Reynolds RC (1997) X‐ray Diffraction and the Identification and Analysis of Clay Minerals. Oxford University Pres sed., New York, Oxford University Press, Oxford, p. 378

Muhammad Faheem MT, Al Bakri AMM, Ghazali CMR, Kamarudin H, Izzat AM & Abdullah A (2013) New Processing Method of Kaolin-Based Geopolymer Brick by Using Geopolymer Brick Machine. Key Engineering Materials, 594–595: 406–410. https://doi.org/10.4028/www.scientific.net/kem.594-595.406

Odom IE (1984) Smectite clay Minerals: Properties and Uses. Philosophical Transactions of the Royal Society: Mathematical, Physical and Engineering Sciences, 311: 391–409. https://doi.org/10.1098/rsta.1984.0036.

Puchulu ME & Fernández D (2014) Características y distribución espacial de los suelos de la provincia de Tucumán. en: Moyano, Puchulu, Fernandez, Vides, Nieva, Aceñolaza (Eds.), Geología de Tucumán. Colegio de Graduados de Ciencias Geológicas de Tucumán, Tucumán pp 240-256

Quiñónez F & Ayala V (2014) Evaluación de la adherencia de revestimientos en paredes construidas con tierra mediante un equipo de laboratorio autoconstruido. Twelfth LACCEI Latin American and Caribbean Conference for Engineering and Technology, Guayaquil. 1-10. http://www.laccei.org/LACCEI2014-Guayaquil/RefereedPapers/RP036.pdf

Randazzo L, Montana G, Hein A, Castiglia A, Rodonò G & Donato DI (2016) Moisture absorption, thermal conductivity and noise mitigation of clay based plasters: The influence of mineralogical and textural characteristics, Applied Clay Science 132–133: 498–507. doi: 10.1016/j.clay.2016.07.021

Sheng G, Johnston CT, Teppen BJ & Boyd SA (2001) Potential contributions of smectite clays and organic matter to pesticide retention in soils, Journal of agricultural and food chemistry, 49 (6): 2899-2907. https://pubs.acs.org/doi/10.1021/jf001485dG.-I

Stazi F, Nacci A., Tittarelli F, Pasqualini E & Munafo P (2016) An experimental study on earth plasters for earthen building protection: the effects of different admixtures and surface treatments, Journal of Cultural Heritage 17:27–41. doi: 10.1016/j.culher.2015.07.009

Van Olphen H (1964) An introduction to Clay colloid chemistry. New York and London (Wiley), 143: 1023-1024. https://doi:10.1180/minmag.1965.035.270.27

Van Olphen H & Fripiat JJ (1979) Data handbook for clay materials and other non-metallic minerals: providing those involved in clay research and industrial application with sets of authoritative data describing the physical and chemical properties and mineralogical composition of the available reference materials, Elsevier Science & Technology ed., California

Downloads

Published

2024-04-29

How to Cite

García Villar, G., Enzo, M. ., & Guillermo, R. . (2024). Clay composition patterns and their influence on the adhesive strength of earthen plasters. Revista De La Construcción. Journal of Construction, 23(1), 71–87. https://doi.org/10.7764/RDLC.23.1.71